86.1313-94—Fuel specifications.

(a) Gasoline fuel. (1) Gasoline having the specifications listed in table N94-1 will be used by the Administrator in exhaust emission testing. Gasoline having these specifications or substantially equivalent specifications approved by the Administrator, shall be used by the manufacturer in exhaust emission testing, except that the octane specification does not apply.
Table N94-1
Item ASTM Value
Octane, research, min D2699 93
Sensitivity, min 7.5
Lead (organic), g/U.S. gal. (g/liter) D3237 1 (0.050) 1 (0.013)
Distillation range:
IBP, °F ( °C) D86 75-95(23.9-35)
10 pct. point, °F ( °C) D86 120-135(48.9-57.2)
50 pct. point, °F ( °C) D86 200-230(93.3-110)
90 pct. point, °F ( °C) D86 300-325(148.9-162.8)
EP, max. °F ( °C) D86 415(212.8)
Sulphur, Max., wt. pct D1266 0.10
Phosphorus, max., g/U.S. gal. (g/liter) D3231 0.005(0.0013)
RVP, psi (kPa) D323 8.0-9.2(60.0-63.4)
Hydrocarbon composition:
Olefins, max. pct D1319 10
Aromatics, max. pct D1319 35
Saturates D1319 (2)
1 Maximum.
2 Remainder.
(2) (i) Unleaded gasoline representative of commercial gasoline which will be generally available through retail outlets shall be used in service accumulation.
(ii) The octane rating of the gasoline used shall not be higher than one Research octane number above the minimum recommended by the manufacturer and have a minimum sensitivity of 7.5 octane numbers, where sensitivity is defined as the Research octane number minus the Motor octane number.
(iii) The Reid Vapor Pressure of the gasoline used shall be characteristic of the motor fuel used during the season in which the service accumulation takes place.
(3) The specification range of the gasoline to be used under paragraph (a) of this section shall be reported in accordance with § 86.094-21(b)(3).
(b) Petroleum diesel test fuel. (1) The petroleum fuels for testing diesel engines employed for testing shall be clean and bright, with pour and cloud points adequate for operability. The petroleum diesel fuel may contain nonmetallic additives as follows: Cetane improver, metal deactivator, antioxidant, dehazer, antirust, pour depressant, dye, dispersant and biocide. Fuels specified for emissions testing are intended to be representative of commercially available in-use fuels.
(2) Petroleum fuel for diesel engines meeting the specifications in Table N94-2, or substantially equivalent specifications approved by the Administrator, shall be used in exhaust emissions testing. The grade of petroleum fuel used shall be commercially designated as “Type 2-D” grade diesel fuel except that fuel commercially designated at “Type 1-D” grade diesel fuel may be substituted provided that the manufacturer has submitted evidence to the Administrator demonstrating to the Administrator's satisfaction that this fuel will be the predominant in-use fuel. Such evidence could include such things as copies of signed contracts from customers indicating the intent to purchase and use “Type 1-D” grade diesel fuel as the primary fuel for use in the engines or other evidence acceptable to the Administrator.
Table N94-2
Item ASTM Type 1-D Type 2-D
Cetane Number D613 40-54 40-48
Cetane Index D976 40-54 40-48
Distillation range:
IBP °F D86 330-390 340-400
( °C) (165.6-198.9) (171.1-204.4)
10 percent point, °F D86 370-430 400-460
( °C) (187.8-221.1) (204.4-237.8)
50 percent point, °F D86 410-480 470-540
( °C) (210-248.9) (243.3-282.2)
90 percent point, °F D86 460-520 560-630
( °C) (237.8-271.1) (293.3-332.2)
EP, °F D86 500-560 610-690
( °C) (260.0-293.3) (321.1-365.6)
Gravity, °API D287 40-44 32-37
Total Sulfur, percent D2622 0.03-0.05 0.03-0.05
Hydrocarbon composition:
Aromatics, pct D1319 or D5186 1 8 1 27
Paraffins, Naphthenes, Olefins D1319 ( 2 ) ( 2 )
Flashpoint, °F D93 120 130
( °C) (48.9) (54.4)
(minimum)
Viscosity, Centistokes D445 1.6-2.0 2.0-3.2
1 Minimum.
2 Remainder.
(3) Petroleum diesel fuel for diesel engines meeting the specifications in table N94-3, or substantially equivalent specifications approved by the Administrator, shall be used in service accumulation. The grade of petroleum diesel fuel used shall be commercially designated as “Type 2-D” grade diesel fuel except that fuel commercially designated as “Type 1-D” grade diesel fuel may be substituted provided that the manufacturer has submitted evidence to the Administrator demonstrating to the Administrator's satisfaction that this fuel will be the predominant in-use fuel. Such evidence could include such things as copies of signed contracts from customers indicating the intent to purchase and use “Type 1-D” grade diesel fuel as the primary fuel for use in the engines or other evidence acceptable to the Administrator.
Table N94-3
Item ASTM Type 1-D Type 2-D
Cetane Number D613 40-56 30-58
Cetane Index D976 Min. 40 Min. 40
Distillation range:
90 pct. point °F ( °C) D86 440-530 (226.7-276.7) 540-630 (282.2-332.2)
Gravity °API D287 39-45 30-42
Total sulfur, min. pct D2622 0.03-0.05 0.03-0.05
Flashpoint, min. °F ( °C) D93 120 (48.9) 130 54.4
Viscosity, centistokes D445 1.2-2.2 1.5-4.5
(4) Other petroleum distillate fuels may be used for testing and service accumulation provided:
(i) They are commercially available; and
(ii) Information, acceptable to the Administrator, is provided to show that only the designated fuel would be used in customer service; and
(iii) Use of a fuel listed under paragraphs (b)(2) and (b)(3) of this section would have a detrimental effect on emissions or durability; and
(iv) Written approval from the Administrator of the fuel specifications must be provided prior to the start of testing.
(5) The specification range of the fuels to be used under paragraph (b) of this section shall be reported in accordance with § 86.094-21(b)(3).
(c) Methanol-fuel. (1) Methanol fuel used for exhaust and evaporative emission testing and in service accumulation of methanol-fueled engines shall be representative of commercially available methanol fuel and shall consist of at least 50 percent methanol by volume.
(i) Manufacturers shall recommend the methanol fuel to be used for testing and service accumulation.
(ii) The Administrator shall determine the methanol fuel to be used for testing and service accumulation.
(2) Other methanol fuels may be used for testing and service accumulation provided:
(i) They are commercially available; and
(ii) Information, acceptable to the Administrator, is provided to show that only the designated fuel would be used in customer service; and
(iii) Use of a fuel listed under paragraph (b)(4)(c)(1) of this section would have a detrimental effect on emissions or durability; and
(iv) Written approval from the Administrator of the fuel specifications must be provided prior to the start of testing.
(3) The specification range of the fuels to be used under paragraphs (c)(1) and (c)(2) of this section shall be reported in accordance with § 86.094-21(b)(3).
(d) Mixtures of petroleum and methanol fuels for flexible fuel vehicles. (1) Mixtures of petroleum and methanol fuels used for exhaust emission testing and service accumulation for flexible fuel vehicles shall consist of the methanol and petroleum fuels listed in paragraph (a) or (b) of this section, and shall be within the range of fuel mixtures for which the vehicle was designed, as reported in accordance with § 86.94-21. The Administrator may use any fuel mixture within this range for testing.
(2) The fuel mixtures used by the manufacturers shall be sufficient to demonstrate compliance over the full design range, and shall include:
(i) For emission testing:
(A) A petroleum fuel specified in paragraph (a) or paragraph (b) of this section;
(B) A methanol fuel representative of the methanol fuel expected to the found in use.
(ii) For service accumulation, an alternating combination of the fuels specified in paragraphs (a) or (b), and (c) of this section that, based on good engineering judgement, demonstrates the durability of the emissions control system. The combination shall be selected such that the cumulative volumes of both the methanol fuel and the petroleum fuel used shall be at least 25 percent of the total fuel volume. The fuels shall be or alternated at intervals not to exceed 500 hours.
(iii) Or, other combinations for testing and/or service accumulation which demonstrate compliance with the standards over the entire design range of the vehicle, provided that written approval is obtained from the Administrator prior to the start of testing.
(3) The specification range of the fuels to be used under this paragraph (d) shall be reported in accordance with § 86.094-21.
(e) Natural gas-fuel. (1) Natural gas-fuel having the following specifications will be used by the Administrator for exhaust and evaporative emission testing of natural gas-fueled engines:
Natural Gas Certification Fuel Specifications
Item ASTM test method No. Value
Methane min. mole pct. D1945 89.0
Ethane max. mole pct. D1945 4.5
C3 and higher max. mole pct. D1945 2.3
C6 and higher max. mole pct. D1945 0.2
Oxygen max. mole pct. D1945 0.6
Inert gases:
Sum of CO2 and N2 max. mole pct. D1945 4.0
Odorant 1
1 The natural gas at ambient conditions must have a distinctive odor potent enough for its presence to be detected down to a concentration in air of not over 1/5 (one-fifth) of the lower limit of flammability.
(2) Natural gas-fuel representative of commercial natural gas-fuel and which will be generally available through retail outlets shall be used in service accumulation.
(3) Other natural gas-fuels may be used for testing and service accumulation provided:
(i) They are commercially available;
(ii) Information, acceptable to the Administrator, is provided to show that only the designated fuel would be used in customer service; and
(iii) Written approval from the Administrator of the fuel specifications must be provided prior to the start of testing.
(4) The specification range of the fuels to be used under paragraphs (e)(1) and (e)(2) of this section shall be reported in accordance with § 86.094-21(b)(3).
(f) Liquified petroleum gas-fuel. (1) Liquified petroleum gas-fuel used for exhaust and evaporative emission testing and in service accumulation shall be commercially available liquefied petroleum gas-fuel.
(i) Manufacturers shall recommend the liquefied petroleum gas-fuel to be used for testing and service accumulation.
(ii) The Administrator shall determine the liquefied petroleum gas-fuel to be used for testing and service accumulation.
(2) Other liquefied petroleum gas-fuels may be used for testing and service accumulation provided:
(i) They are commercially available;
(ii) Information, acceptable to the Administrator, is provided to show that only the designated fuel would be used in customer service; and
(iii) Written approval from the Administrator of the fuel specifications must be provided prior to the start of testing.
(3) The specification range of the fuels to be used under paragraphs (f)(1) and (f)(2) of this section shall be measured in accordance with ASTM D2163-91 and reported in accordance with § 86.094-21(b)(3).
(g) Fuels not meeting the specifications set forth in this section may be used only with the advance approval of the Administrator.

Code of Federal Regulations

[59 FR 48528, Sept. 21, 1994, as amended at 60 FR 34371, June 30, 1995; 62 FR 47125, Sept. 5, 1997]